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Unité Matériaux et Transformations
CNRS UMR 8207 - Université de Lille

UMET - Métallurgie Physique et Génie des Matériaux

Métallurgie Physique et Génie des Matériaux - Scientific instruments

 

Scientific instruments from the UMET instrument database managed by the research group.

3D optical profiler (ContourGT-K 3D Optical Microscope)

3D optical profiler (ContourGT-K 3D Optical Microscope)

Research team: Métallurgie physique et génie des matériaux.

Contact: Ingrid PRORIOL SERRE.

Profilometric measurements by non-contact optical microscope type 3D optical interferometric profilometer for reflective or non-reflective materials
Technical characteristics
  • Measuring range: 2.3mm² to 30μm.
  • Lateral resolution: up to 300 nm
  • Resolution in z: below the nm
 

Atomic Force Microscope Dimension 3100

Research team: Métallurgie physique et génie des matériaux.

Contact: Ingrid PRORIOL SERRE.

Mode: Tapping / contact
Scanners: 90μm x 90μm x-y images, 6μm in vertical imaging (roughness)
Accessories :
  • Anti-vibration table
  • Sample holder: standard 150 mm chuck.
  • Motorized displacement plate (x, y): probed area 125mm x 100mm.
  • MFM mode
 

Atomic Force Microscope Multimode

Research team: Métallurgie physique et génie des matériaux.

Contact: Ingrid PRORIOL SERRE.

AFM Multimode from Veeco
Technical characteristics
  • Contact mode
  • 150μm x 150μm image
  • Vertical scale: 5 μm (roughness)
 
Chamber furnace (1750°C)

Chamber furnace (1750°C)

Research team: Métallurgie physique et génie des matériaux.

Contacts: Franck BéCLIN, Matthieu TOUZIN.

glass synthesis and high temperature annealing
 
cryogenic mill (CryoMill RETSCH)

cryogenic mill (CryoMill RETSCH)

Research team: Métallurgie physique et génie des matériaux.

Contact: Catherine CORDIER.

Vibrating mill, room temperature or liquid nitrogen temperature (77K)
 
Dilatometer DIL 402C

Dilatometer DIL 402C

Research team: Métallurgie physique et génie des matériaux.

Contact: Rajashekhara SHABADI.

Vacuum dilatometer or neutral gas sweeping
Ambient temperature at 1500 ° C
 
Fatigue machine +/- 50 kN

Fatigue machine +/- 50 kN

Research team: Métallurgie physique et génie des matériaux.

Contact: Jean-Bernard VOGT.

Compression / Traction 50 kN with furnace
Fatigue tests on metal test piece
 
fatigue machine with tubular furnace

fatigue machine with tubular furnace

Research team: Métallurgie physique et génie des matériaux.

Contact: Jean-Bernard VOGT.

Compression / Traction 250 kN, furnace max 650°C and possibility induction furnace.
Fatigue tests on metal test pieces up to 10 mm diameter
 
Flash DSC2+ (Mettler Toledo)

Flash DSC2+ (Mettler Toledo)

Research team: Métallurgie physique et génie des matériaux.

Contact: Marie-Noëlle Avettand-Fénoël.

Range of Temperature : T ambient at 1000 °C
Heating rate: 30 K / s to 40000 K/s
Cooling speed in absolute value up to 4000 K/s
 
Forced air annealing furnace (800 ° C)

Forced air annealing furnace (800 ° C)

Research team: Métallurgie physique et génie des matériaux.

Contacts: Franck BéCLIN, Matthieu TOUZIN.

Forced air chamber furnace for non-reducing atmosphere annealing
 
High temperatue differential scanning calorimetry

High temperatue differential scanning calorimetry

Research team: Métallurgie physique et génie des matériaux.

Contact: Rajashekhara SHABADI.

  • High temperature furnace- 700-1500 ° C
  • Low temperature furnace (
  • Possibility of thermal cycling and simulation of rapid cooling
  • Ability to analyze samples under He, Ar and / or N2
 
hot enrobing press

hot enrobing press

Research team: Métallurgie physique et génie des matériaux.

Contacts: Damien CRETON, Matthieu TOUZIN.

Hot enrobing of sample in conductive or non-conductive resins
Coating diameter 30mm,
Enrobing parameters
  • Pressure from 50 to 350 bar in increments of 25 bar
  • Heating time From 1 to 15 minutes. in steps of 0.5 minutes.
  • Heating temperature 80-180 ° C in increments of 5 ° C
  • Cooling time From 1 to 15 min in steps of 0.5 min.
 
Hot press sintering

Hot press sintering

Research team: Métallurgie physique et génie des matériaux.

Contacts: Franck BéCLIN, Matthieu TOUZIN.

Instron 4507, 200 kN cell
Graphite furnace HT 2000 ° C under secondary vacuum or neutral atmosphere (N2, Ar, He, ...)
 
low-pressure plasma system

low-pressure plasma system

Research teams: Ingénierie des systèmes polymères, Métallurgie physique et génie des matériaux.

Contact: Jean-François BRUN.

Low-pressure plasma system with a 40kHz/100W generator for

  • cleaning the surface of most of materials, including the smallest cracks
  • activating the surface to increase wettability

Treatment of small samples (a few cm2 or cm3)

Gaz available: air, pure oxygen.

 
Mössbauer Spectrometry

Mössbauer Spectrometry

Research team: Métallurgie physique et génie des matériaux.

Contact: Catherine CORDIER.

Devices

  • 57Co sources for the study of alloys containing iron;
  • 1 spectrometer for measurements in ambient transmission;
  • 1 spectrometer for reflection measurements at ambient temperature:

                  in CEMS mode - 0.2 μm;
                  in CXMS mode - 2 μm.

Possible Mössbauer studies

  • Identification and determination of phases, determination of their chemical composition;
  • Oxidation state of iron;
  • Local atomic order and local symmetry;
  • Properties: magnetic resolution, indication on charge transfer.


Analyzable materials

  • Powder, solid, sheet or coating on solid;
  • Nature: Steels (with nitrogen) coated (or not), minerals, catalysts, semiconductors.
 
Machine fatigue MTS 100 kN

Machine fatigue MTS 100 kN

Research team: Métallurgie physique et génie des matériaux.

Contact: Jean-Bernard VOGT.

Compression / Traction 100 kN with tubular furnace 650 ° C or mechanical test in liquid nitrogen
Fatigue tests on metal specimen diameter (10 mm) hot or cold
 
Machine fatigue MTS 25 kN

Machine fatigue MTS 25 kN

Research team: Métallurgie physique et génie des matériaux.

Contact: Jean-Bernard VOGT.

Compression / Traction 25 kN
Fatigue tests on small diameter metal specimen (4mm) and thin thickness (of the order of 0.350 mm)
 
Metal Fusion Platform

Metal Fusion Platform

Research team: Métallurgie physique et génie des matériaux.

Contact: David BALLOY.

Development of induction platforms with ATYS Consulting Group
 
Induction furnace 25kW CEIA

     Direct and indirect heating
     Up to 20kg of steel

Resistance Tilting furnace12kW

     10 liters (Al foundry + galvanizing)

+ 1 liter tilting furnace
 
Micro-indenter MHT CSM Instruments

Micro-indenter MHT CSM Instruments

Research team: Métallurgie physique et génie des matériaux.

Contact: Matthieu TOUZIN.

  •  Instrumented indentation (simultaneous recording of force and displacement) for loads ranging from 0.05 to 10 N; not instrumented beyond (up to 30 N)
  • Motorized X-Y stage (positioning
  • Coupled optical observation
  • Vickers type diamond indenter
  • Heated sample plate (up to 450 ° C)
 
mills SPEX 8000 (high energy grinding at ambient temperature)

mills SPEX 8000 (high energy grinding at ambient temperature)

Research team: Métallurgie physique et génie des matériaux.

Contact: Catherine CORDIER.

Possible programming of the duration and grinding cycle;

Container volume about 45 cm3;

grinding vials and balls in steel or alumina
 
Ovens under vacuum (250°C)

Ovens under vacuum (250°C)

Research team: Métallurgie physique et génie des matériaux.

Contacts: Franck BéCLIN, Matthieu TOUZIN.

Oven able to work under primary vacuum.
Capacity 65 l
Max temperature 250°C
 
planetary mill (Fritsch)

planetary mill (Fritsch)

Research team: Métallurgie physique et génie des matériaux.

Contact: Marie-Noëlle Avettand-Fénoël.

Planetary mill used for metalls and mechanical alloying.
 
planetary mill (PM 100 Retsch)

planetary mill (PM 100 Retsch)

Research team: Métallurgie physique et génie des matériaux.

Contacts: Matthieu TOUZIN, Franck BéCLIN.

Planetary mill used for powder metallurgy of ceramic and metal . Mechanical alloying of metals.
Volume of milling jars up to 500 ml.
Possible programming of the duration, the speed and the grinding cycle;
Speed up to 600 rpm;
Bowls and balls in stainless steel, tungsten carbide, agate and alumina.
 
Rolling mill

Rolling mill

Research team: Métallurgie physique et génie des matériaux.

Contacts: David BALLOY, Matthieu TOUZIN.

Mini electric rolling mill
Maximum opening between cylinders: 37 mm
Hot rolling (preheating oven up to 1200 ° C - atmo N2)
Cold rolling
 
tensile test device +/- 30 kN  with +/- 30 kN controlled atmosphere test chamber +/- 30 kN

tensile test device +/- 30 kN with +/- 30 kN controlled atmosphere test chamber +/- 30 kN

Research team: Métallurgie physique et génie des matériaux.

Contact: Jean-Bernard VOGT.

Compression / tensile test 30 kN
Tensile tests or Small Punch Test at temperature up to 500 ° C (heating cord) with control of the oxygen content and moisture content
 
Tensile test device +/- 30kN INSTRON 5567A

Tensile test device +/- 30kN INSTRON 5567A

Research team: Métallurgie physique et génie des matériaux.

Contact: Jean-Bernard VOGT.

Compression / tensile test 30 kN
Tensile tests or Small Punch Test at temperature up to 500 ° C (heating cord)
 
Vibration polisher VibroMet 2 BUEHLER

Vibration polisher VibroMet 2 BUEHLER

Research team: Métallurgie physique et génie des matériaux.

Contact: Damien CRETON.

Finishing polishing with colloidal silica on a wide range of materials, especially for EBSD applications
 
 
UMET - Unité Matériaux et Transformations
CNRS UMR 8207
Université de Lille
Bâtiment C6
59655 Villeneuve d'Ascq
France
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