Physical Metallurgy and Materials Engineering
- Home
- Team directory
- Publications
- Communications
- PhD thesis
- Collaboration network
- Former group members
Equipements
- General database
- Elaboration:
- Characterization:
Research themes
Ongoing projects
- Projet COMASYS
- ANR JCJC RESSET
- ANR MustImplant - Multiscale Smart Texturing of Medical Implants
- PIA ISAC - Innovative System for Actinides Conversion
- Projet européen INNUMAT
Completed projects
- ANR GauguIn
- Interreg SOCORRO2
- Interreg Allihentrop - Synthèse et mise en œuvre de revêtements à base d'ALLIages à Haute ENTROPie
- European project H2020 : GEMMA for GEneration iv Materials MAturity
- Interreg_transport - Réseau TRANSfrontalier pour le développement de revêtements sol-gel POReux sur métaux pour applications Tribologiques
Documents
- Thermodynamique et défauts ponctuels (ADPI)
![UMET - Métallurgie Physique et Génie des Matériaux UMET - Métallurgie Physique et Génie des Matériaux](/Images/vide.gif)
Physical Metallurgy and Materials Engineering - Scientific instruments
Scientific instruments from the UMET instrument database managed by the research group.
![3D optical profiler (ContourGT-K 3D Optical Microscope) 3D optical profiler (ContourGT-K 3D Optical Microscope)](/Instruments/ImagesDB/s_img-164-749740738.jpg)
3D optical profiler (ContourGT-K 3D Optical Microscope)
Research team: Métallurgie physique et génie des matériaux.
Contact: Ingrid PRORIOL SERRE.
- Measuring range: 2.3mm² to 30μm.
- Lateral resolution: up to 300 nm
- Resolution in z: below the nm
Atomic Force Microscope Dimension 3100
Research team: Métallurgie physique et génie des matériaux.
Contact: Ingrid PRORIOL SERRE.
Mode: Tapping / contactScanners: 90μm x 90μm x-y images, 6μm in vertical imaging (roughness)
Accessories :
- Anti-vibration table
- Sample holder: standard 150 mm chuck.
- Motorized displacement plate (x, y): probed area 125mm x 100mm.
- MFM mode
Atomic Force Microscope Multimode
Research team: Métallurgie physique et génie des matériaux.
Contact: Ingrid PRORIOL SERRE.
AFM Multimode from VeecoTechnical characteristics
- Contact mode
- 150μm x 150μm image
- Vertical scale: 5 μm (roughness)
![Chamber furnace (1750°C) Chamber furnace (1750°C)](/Instruments/ImagesDB/s_img-161-370168833.png)
Chamber furnace (1750°C)
Research team: Métallurgie physique et génie des matériaux.
Contacts: Franck BéCLIN, Matthieu TOUZIN.
glass synthesis and high temperature annealing![cryogenic mill (CryoMill RETSCH) cryogenic mill (CryoMill RETSCH)](/Instruments/ImagesDB/s_img-60-91600298.jpg)
cryogenic mill (CryoMill RETSCH)
Research team: Métallurgie physique et génie des matériaux.
Contact: Catherine CORDIER.
Vibrating mill, room temperature or liquid nitrogen temperature (77K)![Dilatometer DIL 402C Dilatometer DIL 402C](/Instruments/ImagesDB/s_img-101-229295526.jpg)
Dilatometer DIL 402C
Research team: Métallurgie physique et génie des matériaux.
Contact: Rajashekhara SHABADI.
Ambient temperature at 1500 ° C
![Fatigue machine +/- 50 kN Fatigue machine +/- 50 kN](/Instruments/ImagesDB/s_img-110-1986974844.jpg)
Fatigue machine +/- 50 kN
Research team: Métallurgie physique et génie des matériaux.
Contact: Jean-Bernard VOGT.
![fatigue machine with tubular furnace fatigue machine with tubular furnace](/Instruments/ImagesDB/s_img-105-943211241.jpg)
fatigue machine with tubular furnace
Research team: Métallurgie physique et génie des matériaux.
Contact: Jean-Bernard VOGT.
Compression / Traction 250 kN, furnace max 650°C and possibility induction furnace.Fatigue tests on metal test pieces up to 10 mm diameter
![Flash DSC2+ (Mettler Toledo) Flash DSC2+ (Mettler Toledo)](/Instruments/ImagesDB/s_img-163-1320049372.jpg)
Flash DSC2+ (Mettler Toledo)
Research team: Métallurgie physique et génie des matériaux.
Contact: Marie-Noëlle Avettand-Fénoël.
Heating rate: 30 K / s to 40000 K/s
Cooling speed in absolute value up to 4000 K/s
![Forced air annealing furnace (800 ° C) Forced air annealing furnace (800 ° C)](/Instruments/ImagesDB/s_img-162-1332443836.png)
Forced air annealing furnace (800 ° C)
Research team: Métallurgie physique et génie des matériaux.
Contacts: Franck BéCLIN, Matthieu TOUZIN.
Forced air chamber furnace for non-reducing atmosphere annealing![High temperatue differential scanning calorimetry High temperatue differential scanning calorimetry](/Instruments/ImagesDB/s_img-100-285158349.jpg)
High temperatue differential scanning calorimetry
Research team: Métallurgie physique et génie des matériaux.
Contact: Rajashekhara SHABADI.
- High temperature furnace- 700-1500 ° C
- Low temperature furnace (
- Possibility of thermal cycling and simulation of rapid cooling
- Ability to analyze samples under He, Ar and / or N2
![hot enrobing press hot enrobing press](/Instruments/ImagesDB/s_img-189-49527894.jpg)
hot enrobing press
Research team: Métallurgie physique et génie des matériaux.
Contacts: Damien CRETON, Matthieu TOUZIN.
Hot enrobing of sample in conductive or non-conductive resinsCoating diameter 30mm,
Enrobing parameters
- Pressure from 50 to 350 bar in increments of 25 bar
- Heating time From 1 to 15 minutes. in steps of 0.5 minutes.
- Heating temperature 80-180 ° C in increments of 5 ° C
- Cooling time From 1 to 15 min in steps of 0.5 min.
![Hot press sintering Hot press sintering](/Instruments/ImagesDB/s_img-61-1838228086.jpg)
Hot press sintering
Research team: Métallurgie physique et génie des matériaux.
Contacts: Franck BéCLIN, Matthieu TOUZIN.
Graphite furnace HT 2000 ° C under secondary vacuum or neutral atmosphere (N2, Ar, He, ...)
![low-pressure plasma system low-pressure plasma system](/Instruments/ImagesDB/s_img-200-1950305495.png)
low-pressure plasma system
Research teams: Ingénierie des systèmes polymères, Métallurgie physique et génie des matériaux.
Contact: Jean-François BRUN.
Low-pressure plasma system with a 40kHz/100W generator for
- cleaning the surface of most of materials, including the smallest cracks
- activating the surface to increase wettability
Treatment of small samples (a few cm2 or cm3)
Gaz available: air, pure oxygen.
![Mössbauer Spectrometry Mössbauer Spectrometry](/Instruments/ImagesDB/s_img-99-600203271.jpg)
Mössbauer Spectrometry
Research team: Métallurgie physique et génie des matériaux.
Contact: Catherine CORDIER.
Devices
- 57Co sources for the study of alloys containing iron;
- 1 spectrometer for measurements in ambient transmission;
- 1 spectrometer for reflection measurements at ambient temperature:
in CEMS mode - 0.2 μm;
in CXMS mode - 2 μm.
Possible Mössbauer studies
- Identification and determination of phases, determination of their chemical composition;
- Oxidation state of iron;
- Local atomic order and local symmetry;
- Properties: magnetic resolution, indication on charge transfer.
Analyzable materials
- Powder, solid, sheet or coating on solid;
- Nature: Steels (with nitrogen) coated (or not), minerals, catalysts, semiconductors.
![Machine fatigue MTS 100 kN Machine fatigue MTS 100 kN](/Instruments/ImagesDB/s_img-107-1187067977.jpg)
Machine fatigue MTS 100 kN
Research team: Métallurgie physique et génie des matériaux.
Contact: Jean-Bernard VOGT.
Compression / Traction 100 kN with tubular furnace 650 ° C or mechanical test in liquid nitrogenFatigue tests on metal specimen diameter (10 mm) hot or cold
![Machine fatigue MTS 25 kN Machine fatigue MTS 25 kN](/Instruments/ImagesDB/s_img-106-1883228198.jpg)
Machine fatigue MTS 25 kN
Research team: Métallurgie physique et génie des matériaux.
Contact: Jean-Bernard VOGT.
Compression / Traction 25 kNFatigue tests on small diameter metal specimen (4mm) and thin thickness (of the order of 0.350 mm)
![Metal Fusion Platform Metal Fusion Platform](/Instruments/ImagesDB/s_img-98-1787547045.jpg)
Metal Fusion Platform
Research team: Métallurgie physique et génie des matériaux.
Contact: David BALLOY.
Direct and indirect heating
Up to 20kg of steel
Resistance Tilting furnace12kW
10 liters (Al foundry + galvanizing)
+ 1 liter tilting furnace
![Micro-indenter MHT CSM Instruments Micro-indenter MHT CSM Instruments](/Instruments/ImagesDB/s_img-102-1869275412.jpg)
Micro-indenter MHT CSM Instruments
Research team: Métallurgie physique et génie des matériaux.
Contact: Matthieu TOUZIN.
- Instrumented indentation (simultaneous recording of force and displacement) for loads ranging from 0.05 to 10 N; not instrumented beyond (up to 30 N)
- Motorized X-Y stage (positioning
- Coupled optical observation
- Vickers type diamond indenter
- Heated sample plate (up to 450 ° C)
![mills SPEX 8000 (high energy grinding at ambient temperature) mills SPEX 8000 (high energy grinding at ambient temperature)](/Instruments/ImagesDB/s_img-97-1223128457.jpg)
mills SPEX 8000 (high energy grinding at ambient temperature)
Research team: Métallurgie physique et génie des matériaux.
Contact: Catherine CORDIER.
Possible programming of the duration and grinding cycle;Container volume about 45 cm3;
grinding vials and balls in steel or alumina
![Ovens under vacuum (250°C) Ovens under vacuum (250°C)](/Instruments/ImagesDB/s_img-167-1502025066.jpg)
Ovens under vacuum (250°C)
Research team: Métallurgie physique et génie des matériaux.
Contacts: Franck BéCLIN, Matthieu TOUZIN.
Oven able to work under primary vacuum.Capacity 65 l
Max temperature 250°C
![planetary mill (Fritsch) planetary mill (Fritsch)](/Instruments/ImagesDB/s_img-59-1461874007.jpg)
planetary mill (Fritsch)
Research team: Métallurgie physique et génie des matériaux.
Contact: Marie-Noëlle Avettand-Fénoël.
Planetary mill used for metalls and mechanical alloying.![planetary mill (PM 100 Retsch) planetary mill (PM 100 Retsch)](/Instruments/ImagesDB/s_img-58-1611997878.jpg)
planetary mill (PM 100 Retsch)
Research team: Métallurgie physique et génie des matériaux.
Contacts: Matthieu TOUZIN, Franck BéCLIN.
Speed up to 600 rpm;
Bowls and balls in stainless steel, tungsten carbide, agate and alumina.
![Rolling mill Rolling mill](/Instruments/ImagesDB/s_img-62-1929733309.jpg)
Rolling mill
Research team: Métallurgie physique et génie des matériaux.
Contacts: David BALLOY, Matthieu TOUZIN.
Maximum opening between cylinders: 37 mm
Hot rolling (preheating oven up to 1200 ° C - atmo N2)
Cold rolling
![tensile test device +/- 30 kN with +/- 30 kN controlled atmosphere test chamber +/- 30 kN tensile test device +/- 30 kN with +/- 30 kN controlled atmosphere test chamber +/- 30 kN](/Instruments/ImagesDB/s_img-108-613952818.jpg)
tensile test device +/- 30 kN with +/- 30 kN controlled atmosphere test chamber +/- 30 kN
Research team: Métallurgie physique et génie des matériaux.
Contact: Jean-Bernard VOGT.
Compression / tensile test 30 kNTensile tests or Small Punch Test at temperature up to 500 ° C (heating cord) with control of the oxygen content and moisture content
![Tensile test device +/- 30kN INSTRON 5567A Tensile test device +/- 30kN INSTRON 5567A](/Instruments/ImagesDB/s_img-109-1615278036.jpg)
Tensile test device +/- 30kN INSTRON 5567A
Research team: Métallurgie physique et génie des matériaux.
Contact: Jean-Bernard VOGT.
![Vibration polisher VibroMet 2 BUEHLER Vibration polisher VibroMet 2 BUEHLER](/Instruments/ImagesDB/s_img-191-1943546913.jpg)
Vibration polisher VibroMet 2 BUEHLER
Research team: Métallurgie physique et génie des matériaux.
Contact: Damien CRETON.
Finishing polishing with colloidal silica on a wide range of materials, especially for EBSD applications